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Ingeo Polylactic Acid (PLA) 3D870

    • Product Name: Ingeo Polylactic Acid (PLA) 3D870
    • Factroy Site: No. 100, Qinhuai Road, Jiangning District, Nanjing, Jiangsu, China
    • Price Inquiry: sales4@ascent-chem.com
    • Manufacturer: Boxa Chemical Group Ltd
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    Specifications
    HS Code 214696
    Chemicalname Polylactic Acid
    Grade 3D870
    Density 1.24 g/cm³
    Meltflowrate 15 g/10 min (210 °C, 2.16 kg)
    Meltingpoint 165-180 °C
    Glasstransitiontemperature 55-60 °C
    Tensilestrength 60 MPa
    Tensilemodulus 3.5 GPa
    Elongationatbreak 4%
    Flexuralstrength 90 MPa
    Flexuralmodulus 3.5 GPa
    Notchedizodimpact 2.5 kJ/m²
    Heatdeflectiontemperatureat0 45mpa 120 °C
    Heatdeflectiontemperatureat1 82mpa 90 °C
    Vicatsofteningpoint 60 °C
    Biobasedcontent 100%
    Printtemperature 210-230 °C
    Bedtemperature 40-60 °C

    As an accredited Ingeo Polylactic Acid (PLA) 3D870 factory, we enforce strict quality protocols—every batch undergoes rigorous testing to ensure consistent efficacy and safety standards.

    Packing & Storage
    Packing Ingeo Polylactic Acid (PLA) 3D870 is supplied in 25 kg moisture-barrier foil-lined bags, palletized and stretch-wrapped for shipment.
    Container Loading (20′ FCL) Ingeo PLA 3D870 loaded in a 20′ FCL container, palletized, securely strapped, and shrink-wrapped for safe ocean transport.
    Shipping Ingeo Polylactic Acid (PLA) 3D870 is not classified as dangerous goods for transport. Ship in sealed moisture-barrier packaging, cool and dry, away from heat and moisture. No UN number, hazard class, or special labels required. Handle as non-hazardous thermoplastic resin; follow local regulations and supplier SDS.
    Storage Store Ingeo Polylactic Acid (PLA) 3D870 in a cool, dry, well-ventilated area. Keep containers tightly closed in original moisture-barrier packaging with desiccant. Protect from heat, direct sunlight, and ignition sources. Avoid strong oxidizing agents. Recommended storage: 10–30°C and relative humidity below 50%. Reseal opened packages promptly; moisture exposure can degrade filament/resin quality. Keep away from incompatible materials.
    Shelf Life Store in a cool, dry place in sealed packaging; shelf life is 12 months when protected from moisture and heat.
    Application of Ingeo Polylactic Acid (PLA) 3D870
    Application screening for Ingeo PLA 3D870 divides along four conversion routes: monofilament extrusion for fused filament fabrication, post-print annealing for load-bearing assembly aids, sacrificial pattern burnout in investment casting, and filled-compound deposition for stiffness-critical fixturing. The resin is a crystallizable polylactic acid with an elevated melt strength and impact response relative to unmodified PLA; downstream qualification is controlled by residual moisture, melt residence time, and the thermal history of the printed shell. No single set of mechanical properties applies across all routes because the amorphous printed state and the semi-crystalline annealed state produce divergent ASTM D638-14 and ISO 527-2 results. The following scenarios treat separate conversion routes, not generic PLA handling practices.

    Why does monofilament ovality drift outside 1.75 ± 0.03 mm when the melt pump is omitted from a 32:1 L/D line?

    After incoming resin has been dried in a desiccant dryer with a dew point ≤ -40 °C for 4 h at 80 °C to reduce moisture below 250 ppm, the granules are fed to a single-screw extruder with L/D of 28:1 to 32:1 and a compression ratio of 2.8:1 to 3.2:1. Barrel set points from feed to metering are 180 °C, 195 °C, 205 °C, and 210 °C; the die is held at 205 °C, and melt temperature at the adapter is maintained at 195–210 °C. The hopper throat is water-cooled to 40–50 °C to prevent pellet bridging. A 40/60 stainless steel screen pack is placed before a positive-displacement melt pump; the pump suction pressure is controlled at 30–40 bar and discharge pressure at 80–120 bar. Without the melt pump, single-screw pressure pulsation of 1–2% maps directly to filament diameter variation of 0.04–0.08 mm and is visible as periodic ovality. Closed-loop control of melt pump speed and a dual-axis laser diameter gauge sampling at 500 Hz is required to hold the 1.75 mm or 2.85 mm nominal diameter within ±0.03 mm and ±0.05 mm respectively.

    The vertical melt strand enters a water quench bath controlled at 50–60 °C. Water below 50 °C freezes the surface into an amorphous skin too quickly and produces residual stress; water above 60 °C allows the strand to sag and increases ovality beyond 0.05 mm. The line uses a draw ratio of 2.5:1 to 3.5:1 between the first and second godet stand; an air wipe removes entrained water before the laser gauge and winding. Winding tension is kept at 0.5–1.5 N for 1.75 mm filament. Residual moisture above 250 ppm triggers hydrolytic chain scission in the barrel; melt viscosity falls below the datasheet 9–12 g/10 min melt flow range measured under ISO 1133-1:2022 at 210 °C and 2.16 kg, and melt strength collapses. Polymer temperature exceeding 240 °C for more than 5 min depolymerizes PLA, generating lactide and acetaldehyde; the filament develops bubbles and intermittent draw breaks.

    Ingeo 3D870 is sensitive to ambient humidity above 60% RH; pellets exposed for more than 30 min should be re-dried. The failure mode observed on production lines is not a gross diameter failure but a slow shift in melt viscosity that changes draw resonance frequency, producing a sinusoidal filament diameter trace. The winding station alarm thresholds are set at ±0.04 mm for 1.75 mm filament and ±0.06 mm for 2.85 mm filament; continuous spools outside these limits are rejected because downstream FFF extruders cannot maintain constant melt pressure with oval feedstock.

    In electronics manufacturing cells, flatness-critical assembly nests and robotic gripper fingers printed from 3D870 are subjected to post-print annealing before release to an SMT line. The dominant failure mode is not print delamination but annealing distortion caused by non-uniform crystallinity across the Z-axis. A typical nest is printed with a 0.15 mm layer height, four perimeter walls, 40% gyroid infill, a bed temperature of 60 °C, and no heated enclosure. The as-printed shell remains mostly amorphous because the melt is cooled below the glass transition of 55–60 °C within seconds; this state yields higher impact but lower heat deflection than the annealed state. Heat deflection under 0.455 MPa as printed is typically 52–56 °C per ASTM D648-18 Method B; that is insufficient for jigs that contact 70–90 °C reflow fixtures or curing ovens.

    Annealing in a forced-air oven at 85–100 °C for 30–60 min raises the degree of crystallinity and shifts the 0.455 MPa HDT to 80–95 °C. The part must be constrained in a rigid aluminium or filled-epoxy fixture because PLA softens when the oven temperature crosses the glass transition; unsupported flat plates curl at corners and contract unevenly. Dimensional compensation factors of 0.4–0.8% in the XY plane and 0.2–0.5% in Z are applied before printing; the actual value depends on infill ratio, wall count, and anneal temperature. Oven ramp rates above 2 °C/min create shell-core temperature gradients and visible sink marks above thick infill ribs. After annealing, the fixture body exhibits higher HDT but lower notched Izod impact than the amorphous printed condition; the technical data sheet values for dry as-moulded plaques do not capture this trade-off. Qualification therefore requires printed test coupons made in the same orientation and annealing fixture as the production part. Z-axis tensile strength can be 30–50% lower than XY-plane values because of interlayer adhesion limits. Holes and snap-fit slots are machined after annealing whenever positional tolerance is tighter than ±0.10 mm.

    Low-ash pattern burnout and the ceramic shell expansion limit during foundry trials

    At investment casting foundries, patterns printed from 3D870 are used for short-run steel and aluminium castings where pattern tooling cost is prohibitive. The pattern is printed with minimal infill (10–15% gyroid or square) to reduce ash residue and expansion force during burnout. The outer shell is sealed with a thin coating of foundry wax or polyvinyl alcohol to prevent ceramic slurry absorption. Ceramic shell build follows standard alternate dip coats with zircon and fused silica, with an initial prime coat thickness of 200–400 µm. The pattern configuration must include internal vents and drain holes to channel gas evolution; closed-cell infill traps gas and the ceramic shell cracks at internal corners. Burnout begins with a slow ramp from ambient to 150 °C at 0.5–1 °C/min, then passes through the PLA softening range near 55–100 °C, followed by decomposition between 250 °C and 450 °C. The largest risk is shell cracking caused by polymer expansion before decomposition; autoclave or flash-fire wax removal used for wax patterns cannot be used directly because PLA has no wax flow phase.

    Residual ash after burnout at 700–800 °C under air is low for PLA-based formulations, but additives in 3D870 may leave inorganic residues; the furnace must be vented and the shell held at 700 °C for at least 1 h to oxidize carbon. Incomplete burnout produces carbon defects in ferrous castings. Published data for the specific expansion rate of 3D870 in a ceramic shell is limited; foundries should run a shell survivability test on a representative lattice before committing production patterns. The printed pattern is often coated with a microcrystalline wax to produce a positive expansion buffer and improve the dewax path before the PLA decomposes. This is an operational boundary, not a general-purpose substitute for wax pattern material.

    When stiffness-driven replacement of aluminium end-of-arm tooling is under consideration, direct printing with unfilled 3D870 rarely meets flexural modulus above 3,000 MPa; a task-specific compound is prepared by melt-mixing 10–15 wt% chopped carbon fibre or 15–20 wt% short glass fibre into the resin on a co-rotating twin-screw extruder with L/D of 40:1 and screw speed of 300–400 rpm. Barrels are set at 170–200 °C and vacuum devolatilization at -0.08 MPa removes moisture and polar oligomers. Throughput is set to maintain melt temperature below 210 °C. Coupling agents such as maleic anhydride-grafted PLA at 1–2 wt% improve fibre-resin adhesion, but published data for this specific configuration is limited; compounders should prepare tensile and flexural bars under ISO 527-2 and ISO 178 before designing tool geometry. The compound is deposited through a pellet-fed screw pump or a large-format FFF hot end with nozzle orifice of 0.8–1.2 mm. Nozzle temperature is maintained at 200–210 °C; higher temperatures accelerate PLA chain scission but improve fibre wetting.

    The printed tool body is annealed at 90 °C for 60 min to raise heat deflection, then post-machined to flatness below 0.05 mm/m. Carbon fibre raises flexural modulus to 5,000–7,000 MPa in the XY plane while reducing interlayer peel strength; measured Z-axis strength may fall below 30 MPa. Therefore the tooling is designed as a printed blank with machined pockets rather than a direct net-shape part. Sharp internal radii are machined, because the fibre-filled printed contour has sufficient material but poor surface roughness; the printed contour itself is only a preform.

    Semi-crystalline annealed parts and the loss of impact-induced ductility are evaluated in low-volume medical device fixture frames and inspection gauges. The annealed 3D870 part shows higher hardness and better resistance to cutting oils, but the crystallized matrix becomes more brittle than as-printed amorphous material; notched Izod impact measured under ISO 180/A may drop by 20–40% after a 90 °C anneal. Gauges and frames should not rely on press-fit pins into annealed holes; reaming or a helicoil insert is used to avoid hoop stress cracks. The operational limit is set at 60 °C continuous service for annealed unfilled 3D870 under load-bearing applications, with short excursions to 90 °C valued only for zero-load dimension checks. Published data for long-term creep of annealed 3D870 under load is limited; designers should quantify creep by ISO 899-2 on printed coupons before specifying this grade in continuous-fixture service.

    Short-run consumer electronics enclosure prototypes made from 3D870 are evaluated against polycarbonate-acrylonitrile butadiene styrene blends for drop impact and snap-fit insertion. Material selection is not based on datasheet notched Izod alone; printed wall thickness, raster angle, and moisture state before printing dominate the final impact result. For a two-part enclosure with wall thickness 2–3 mm, the printing profile uses nozzle temperature 205 °C, bed temperature 60 °C, extrusion width 0.45 mm, and raster angle ±45° on alternating layers. Sharp interior corners below 0.5 mm radius act as stress raisers; snap-fit hooks are thickened to 1.2–1.5 mm and printed in the XY plane to avoid Z-layer cleavage. Prototype drop tests at 0.5 m and 1.0 m onto concrete produce different failure modes: dry pellets print parts that survive the lower energy case, but repeated impacts at 1.0 m propagate cracks along layer lines unless the part is annealed or coated.

    Compliance requirementStandard or clauseSpecimen conditionAction for 3D870 enclosure prototype
    Flexural modulusISO 178Annealed printed XY couponReport printed value separate from as-moulded datasheet
    Notched Izod impactISO 180/ADry as-printed and annealedTest both states; orientation dependence is significant
    Heat deflectionASTM D648-18 Method BAnnealed printedUse 0.455 MPa for jig limitations; 1.82 MPa value lower
    FlammabilityUL 94Finished enclosureBaseline material not V-0; coating or compound required

    Regulatory checks for consumer electronics prototypes are tied to RoHS Directive 2011/65/EU Annex II and REACH Regulation (EC) No 1907/2006 SVHC Candidate List obligations on the finished article. Flame-retardant performance is not an inherent property of 3D870; enclosures requiring UL 94 V-0 must receive a post-print coating or use a compounded flame-retardant variant. The material is hygroscopic; enclosures stored in non-conditioned environments absorb moisture above 0.3% and can blister during subsequent heat staking or ultrasonic welding. Pre-drying at 50–60 °C for 12 h is required before any secondary thermal joining operation. Isopropyl alcohol cleaning causes environmental stress cracking if printed parts are under flexural load; operators should use dry polypropylene bristle brushes or inert gas duster for cleaning printed enclosures. Annealed 3D870 shows better resistance to aliphatic hydrocarbons but does not withstand methyl ethyl ketone, toluene, or esters.

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    Certification & Compliance
    More Introduction

    Ingeo PLA 3D870, supplied by NatureWorks, is a polylactic acid resin within the Ingeo additive-manufacturing portfolio and is specified for fused filament fabrication where printed components are expected to tolerate intermittent exposure to elevated temperatures without excessive deformation. The grade is formulated with a controlled D-lactide fraction and a nucleation package that permits cold crystallization during post-print annealing. A melt mass-flow rate of 9–12 g/10 min at 210 °C/2.16 kg (ISO 1133-1:2022) and a nominal solid density of 1.24 g/cm³ (ISO 1183-1:2019) place the resin in the medium-flow range for PLA. Compared with standard PLA filament grades such as Ingeo 3D850, the 3D870 is formulated to provide a higher post-annealed heat deflection temperature, reduced in-print warpage, and more consistent layer bonding, but these advantages are retained only when the material is dried below the supplier moisture threshold and annealed within a narrow thermal cycle.

    When Does Moisture Tolerance Limit Melt Processing?

    PLA is a polyester that undergoes hydrolytic chain scission when processed with residual moisture above a critical concentration. For Ingeo PLA 3D870, the moisture content prior to extrusion should be reduced to below 250 ppm, preferably below 150 ppm. Drying in a desiccant dryer at 60 °C for 4 h is commonly sufficient when inlet dew point is maintained at or below -40 °C. If ambient relative humidity exceeds 60%, open-air feed hoppers should not be used because the resin can re-absorb surface moisture within 20–30 min and produce filament with internal voids, surface roughness, or diameter drift. Hydrolytic degradation is observable as a rise in melt flow rate at fixed temperature and a reduction in melt strength at the die. On production lines, moisture-related MFR drift of 1–2 g/10 min can shift die pressure by 8–15% and require adjustment of barrel zone set points.

    Single-screw extrusion of 3D870 into filament is typically performed on a 24:1 to 30:1 L/D extruder with a general-purpose screw having a compression ratio of 2.5:1 to 3.0:1. Barrel temperatures from feed to metering zone generally range from 170 °C to 210 °C, with the die and melt temperature held at 190–220 °C. Melt temperature should not exceed 230 °C for more than 5 min because thermal depolymerization generates lactide and discoloration. Water-ring or vacuum sizing of the monofilament is possible, but the strand must be cooled gradually to avoid amorphous orientation that later relaxes during printing. Filament diameter is maintained at 1.75 ± 0.05 mm or 2.85 ± 0.05 mm; ovality above 0.03 mm can cause inconsistent feed force in Bowden or direct-drive extruders.

    For compounded variants, twin-screw extrusion on a 40:1 L/D co-rotating line with atmospheric and vacuum venting is used. Vacuum vent pressure below -0.08 MPa is recommended when pigments, impact modifiers, or mineral fillers are incorporated. Because the crystallization half-time of PLA shortens sharply between 90 °C and 120 °C, barrel zones downstream of the vent should not remain in that temperature range for long residence periods, otherwise crystalline domains may form and produce die lip buildup.

    Mechanical property data for Ingeo PLA 3D870 are typically generated on dry, annealed or injection-molded specimens. The following supplier-reported nominal values provide a baseline for material selection and should be verified against the production lot certificate:

    Nominal supplier-reported physical properties for unfilled Ingeo PLA 3D870
    PropertyNominal valueTest method
    Melt mass-flow rate9–12 g/10 min at 210 °C/2.16 kgISO 1133-1:2022
    Density1.24 g/cm³ISO 1183-1:2019
    Tensile yield strength48 MPaASTM D638-14
    Tensile modulus3300 MPaASTM D638-14
    Flexural strength83 MPaISO 178:2019
    Flexural modulus2900 MPaISO 178:2019
    Notched Izod impact18 J/mASTM D256-10
    Heat deflection temperature85 °C at 0.455 MPa, annealedISO 75-2:2013, Method B
    Glass transition temperature55 °CISO 11357-1:2016, DSC
    Melting temperature155 °CISO 11357-1:2016, DSC

    The tensile modulus of approximately 3300 MPa places 3D870 near the upper stiffness range for unfilled PLA and above most PETG filament grades. However, the notched Izod value remains below typical ABS values, so the material should not be selected for sharp-cornered load-bearing parts subject to impact. The heat deflection temperature of 85 °C at 0.455 MPa applies only after annealing; as-printed amorphous PLA parts may deflect at temperatures closer to the glass transition near 55 °C. Published data for printed part properties of 3D870 are more limited than data for molded specimens, and print-orientation effects must be characterized for structurally loaded designs.

    When Annealing Is Required to Reach the Upper Service Temperature

    As-printed FFF parts cool rapidly and contain a predominantly amorphous PLA matrix. The upper service temperature is therefore governed by the glass transition near 55 °C, not by the crystalline melting point. To exploit the higher heat deflection temperature of 3D870, printed parts must be annealed in a forced-convection oven at 80–95 °C for 30–60 min, followed by slow cooling at or below 1 °C/min. The annealing step increases crystalline fraction above approximately 35%, shifting the heat deflection temperature toward the supplier-reported 85 °C at 0.455 MPa. Annealing also relieves some internal stress but introduces anisotropic shrinkage, typically 0.5–2.0% in the build plane and less in the Z direction depending on infill density and perimeter count.

    Parts with large flat sections require fixturing during annealing because the cold-crystallization exotherm can induce warpage before the part reaches uniform temperature. A heated chamber or constrained flat plate is preferred when part thickness exceeds 8 mm. The annealing window is narrow: below 75 °C crystallization is slow, while above 100 °C the part softens before sufficient crystallinity develops. In multi-material assemblies, metal inserts or dissimilar polymer cores should be avoided unless the assembly can tolerate differential thermal expansion. Published process data for specific oven loadings and part geometries are limited, so production-scale annealing cycles should be validated by differential scanning calorimetry of the printed wall rather than by visual inspection alone.

    When printing before annealing, a nozzle temperature of 200–230 °C and a build plate temperature of 50–70 °C are typical. A heated bed is required to control first-layer adhesion and reduce part lift. Enclosed build chambers are not mandatory for small parts, but parts longer than 150 mm benefit from chamber temperatures of 35–45 °C to suppress differential shrinkage. Part cooling fans should be reduced or disabled for the first 3–5 layers and limited thereafter to preserve interlayer fusion. Because PLA is shear-thinning, print speeds above 80 mm/s can reduce melt residence time in the nozzle and lower layer adhesion; larger nozzles or higher melt temperatures within the specified window may be required at higher linear speeds.

    Differences from other products become most apparent in thermal and processing behavior. Compared with Ingeo 3D850, 3D870 has a more aggressive crystallization package and typically lower warpage in large-format prints, but it also demands tighter drying discipline and a more deliberate annealing cycle. Compared with ABS, 3D870 prints at 20–30 °C lower nozzle temperature, does not require a high-temperature chamber for most geometries, and produces no styrene odor, but its impact toughness and continuous-use temperature under load remain lower. Compared with PETG, 3D870 has higher tensile stiffness and better self-supporting behavior, but lower elongation at break and greater sensitivity to moisture-induced hydrolysis during storage and processing.

    Operational boundaries for Ingeo PLA 3D870 include the following: storage in sealed containers at 20–30 °C and below 60% RH; drying before every extrusion or printing conversion; avoidance of melt residence above 230 °C for more than 5 min; and avoidance of repeated extrusion cycles because cumulative molecular weight loss shifts melt flow upward and reduces impact resistance. The resin is not recommended for continuous immersion in boiling water, steam sterilization, or prolonged outdoor weathering without UV stabilization. Chemical exposure to strong alkalis, chlorinated solvents, and concentrated acids causes surface erosion or bulk degradation. For electrical and electronic equipment applications, the unfilled resin is generally expected to meet the substance restrictions of RoHS Directive 2011/65/EU, but compounded grades containing pigments, flame retardants, or antistatic additives require supplier-specific compliance verification. Food-contact status must be confirmed for the specific article and use condition; the resin should not be assumed to be food-contact approved solely because it is bio-based.